Soma Chakraborty, Jayanta Chattopadhyay, Wenhua Guo, and W. Edward Billups*
Angew. Chem. Int. Ed. 2007, 46, Early View published on May 3, 2007.
Point: C8K is a long-investigated material good for catalysis from potassium intercalation with graphite. Now C8K can be used as precursor to prepare soluble (exfoliated) graphenes.
Synthesis:
Organic-soluble:
![](https://blogger.googleusercontent.com/img/b/R29vZ2xl/AVvXsEjYGHZZwOxicfNfU0BGWDIoTSM6Jdu_ogLxS3sJ8SP0kNt14iEVkNLVdhjDLZVG4lLWa4mbNbmDDWZvhzr9-PLMgDonp2_iJ-QBfY-tyX4McDsifudixxI7BonTAzWd9tGGi5gUarCXXnwQ/s400/Figure+1.jpg)
Water-soluble:
![](https://blogger.googleusercontent.com/img/b/R29vZ2xl/AVvXsEjtd6szBdUQvqI8Wyi_Sy_hzzRJhYDJRbKxxVXrkKjd7Ui1sR39BvBiFvAr6Kpshg0FZV_xb2gVFrYFJQtDQshRClRjTeJAMRIUbc7wvKDCnhQour4lAA5UEj8psCGFUW1TPMsBRR5Su_HC/s400/Figure+2.jpg)
Characterization:
Raman: Much increased D-band after functionalization.
![](https://blogger.googleusercontent.com/img/b/R29vZ2xl/AVvXsEgAkVPFcFAVWvjlNvDrsgm7516qbHybKJEKpw1q5QGq5dXo69SJwVEAsoqwFdwYI2SPFZiQfKIpxBIhmtmZkCNEpxHoX8x8D7E3DyX5gXyGPH5CIB7xRVh4nWm6RtCpf5gsPrxx04pAAlT_/s400/Figure+4.jpg)
TGA (Ar/10C/min/800C): 15% loss (one dodecyl per 78 graphite carbons)
FT-IR: C-H; C=O; N-H.
XPS: Presence of N.
TEM: Bumps on graphite surface = functionalities; 6-20 layers; ~100 nm in size (Tag: Can we see potassium?)
![](https://blogger.googleusercontent.com/img/b/R29vZ2xl/AVvXsEggqg6IIBB9seMkBYCze1hPP2dBrC2P0NiB6K8tWXkuMbrtqEO_8AUCbENK4ghyHZN0uWlG8HhvfrDqhFL_ijX-86mRspHycw7RYHmt_N9kLan7xqFpYGUukBpyr3b7v0WVO3cEs6xt516E/s400/Figure+3.jpg)
AFM: height (30%: 2-4 nm; 70%: 7-9 nm); size: 0.1-1.4 microns.
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